GH2070P合金在持久过程中的组织演变分析

    Analysis of Microstructure Evolution of GH2070P Alloy During High Temperature Creep-rupture Test

    • 摘要: 对650 ℃超超临界锅炉用候选材料GH2070P合金管在675 ℃进行不同应力水平的高温持久试验,基于等温线法预测10万h的高温持久强度,分析了不同高温持久时间的微观组织演变情况和断口情况。研究发现,基于目前的试验数据,热轧GH2070P合金管在675 ℃温度外推10万h 的持久强度为141 MPa,满足设计目标要求;随着持久时间的增加,γ′相尺寸逐渐粗化,符合LSW规律。大量弥散分布的球状γ′相对位错有很强的钉扎作用,使GH2070P合金具有较好的高温强度和持久强度;晶界析出断续的M23C6型碳化物,未形成网状结构;高温持久试验断口表现为高温蠕变导致的沿晶断口,在试样沿晶断裂时发生了微观上的塑性变形。

       

      Abstract: An investigation is conducted on the candidate material GH2070P alloy tube for the 650 ℃ ultra supercritical boiler service by performing the high-temperature creep rupture tests at 675 ℃ under various stress levels. The isothermal method is employed to predict the 100 000 h high-temperature creep strength. The microstructure evolution and the fracture characteristics at different durations of high-temperature creep are analyzed. It is revealed via the study that based on the existing data from the test the extrapolated 100 000 h creep strength of the GH2070P alloy tube at 675 ℃ is 141 MPa,meeting the design target requirements;along with the increase of the creep duration,the size of γ′ phase gradually coarsens,conforming to the LSW law;a great number of finely dispersed spherical γ′ phases have a strong pinning effect on the relative dislocations,providing the GH2070P alloy with good high-temperature strength and creep strength;the M23C6 carbides precipitated at the grain boundary in the GH2070P alloy form no network structure;the fracture surfaces of the GH2070P alloy after the high-temperature creep-rupture tests exhibit intergranular fractures as caused by the hi-temperature creep accompanied by micro-plastic deformation during the intergranular fracture of the specimens.

       

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